WitrynaA 1-L, round-bottomed flask with a magnetic stirrer bar is charged with (2R,4R)-1,5-dichloro-2,4-pentanediol (6.00 g, 34.7 mmol) and diethyl ether (270 mL), and the …

Organic Syntheses Procedure

WitrynaThe one-hole rubber septum used for the transfer process was obtained by using a cork bore of the appropriate size on a 24/40 rubber septum (Aldrich Chemical Company, … WitrynaThe reaction is diluted with saturated aqueous NH 4 Cl solution (300 mL), and the resulting solution is transferred to a 1-L separatory funnel. The aqueous phase is separated and extracted with diethyl ether (3 x 100 mL). The combined organic layers are washed sequentially with 10% aqueous HCl solution (200 mL) and saturated NaCl … the mark condominium association

SUPPORTING INFORMATION - pubs.acs.org

http://www.orgsyn.org/demo.aspx?prep=V77P0220 WitrynaA 250-mL, three-necked, round-bottomed flask is equipped with a mechanical stirrer, a reflux condenser fitted with a drying tube, and a stopper. The flask is charged with 14.3 g (0.1 mol) of 5-(2-hydroxyethyl)-4-methyl-1,3-thiazole, 12.7 g (0.1 mol) of freshly distilled benzyl chloride, and 50 mL of dry acetonitrile.The mixture is heated at reflux for 24 hr … WitrynaOrganic Syntheses, Inc ., its Editors, and its Board of Directors do not warrant or guarantee the safety of individuals using these procedures and hereby disclaim any liability for any injuries or damages claimed to have resulted from or related in any way to the procedures herein. 3. Discussion tiered herb containers